As is the life of most organometallic chemists, analysis by NMR involves several additional steps compared to chemistry done at the bench. For example, once you’ve performed a reaction in a glovebox, you need to take some special precautions to make sure that air doesn’t leach into your NMR tube once it comes out of the antechamber. Most people will either use septa combined with parafilm to prevent air from seeping in, or some may use Teflon-sealed “J-Young” tubes (Fig. 3[4]) if their complex is really air-sensitive. Then it’s the drawn-out process of: Withdraw your sample through the antechamber, go to the NMR in the basement, obtain spectra, come back to the lab, and cycle it back into the glovebox via the antechamber if required. A royal pain? You bet.